⛽ CFPP — Cold Filter Plugging Point

Petrochemistry PN-EN 116

In short

Determination of the cold filter plugging point (CFPP) of diesel fuels and domestic heating fuels: the sample is cooled stepwise and at every 1 °C drawn through a standardized wire mesh filter under a vacuum of 2 kPa. The test is performed according to PN-EN 116:2015-09; Definition of CFPP: highest temperature at which the fuel fails to pass through the filter in a specified time (3.1). The procedure comprises 5 steps; it is used for: Diesel fuel — CFPP at most 0 / −10 / −20 °C in the summer, transitional and winter periods; with improved low-temperature properties −32 °C (Journal of Laws 2024, item 1018), Methyl ester used as a stand-alone fuel — 0 / −10 / −20 °C (Journal of Laws 2025, item 426, Annex 1), Domestic heating fuels, distillate fuels, paraffinic diesel fuels, including those with FAME, flow improvers and other additives (clause 1).

At a glance

  • Standard: PN-EN 116:2015-09
  • Category: Petrochemistry
  • Procedure steps: 5
  • Definition of CFPP: highest temperature at which the fuel fails to pass through the filter in a specified time (3.1)
  • Temperature step: filtration at every 1 °C (clause 4)
  • Vacuum: 2 kPa (clause 4)

Overview

STATUS (as of 30.10.2026). PN-EN 116:2015-09 — Polish version, published 29.09.2016, implements EN 116:2015 [IDT]; it replaced PN-EN 116:2001. The PKN catalogue card has no withdrawal note — the standard is current; Polish title according to the card: “Oleje napędowe i oleje opałowe lekkie — Oznaczanie temperatury zablokowania zimnego filtru — Metoda stopniowego schładzania”. EN 116:2015 replaced EN 116:1997: the automated method is described in detail alongside the former manual procedure, and the scope and precision were changed after a European interlaboratory study that also covered FAME and FAME blends in diesel fuel. An alternative technique with a linear cooling bath is EN 16329.

DEFINITION AND PRINCIPLE (3.1, clause 4). The CFPP is the highest temperature at which a given volume of fuel fails to pass through a standardized filtration device in a specified time, when cooled under standardized conditions. A test portion of the fuel is cooled and, at intervals of 1 °C, drawn into a pipette under a controlled vacuum of 2 kPa through a standardized wire mesh filter. The test continues until the wax crystals that have separated stop or slow down the flow so that filling the pipette takes longer than 60 s or the fuel fails to return completely to the test jar before it has cooled by a further 1 °C. The indicated temperature at which the last filtration was commenced is recorded as the CFPP.

SCOPE (clause 1). Diesel and domestic heating fuels: FAME, distillate fuels and paraffinic diesel fuels, including those containing FAME, flow improvers or other additives. The test is carried out with automated equipment; manual equipment may be used, but for referee purposes only automated equipment is allowed. The result is used to estimate the lowest temperature at which a fuel gives trouble-free flow in the fuel system; for diesel fuels it is usually close to the temperature of failure in service, except when the system contains a paper filter exposed to the weather or the CFPP is more than 12 °C below the cloud point. Domestic heating installations are usually less critical. The difference between results for the sample as received and after heat treatment at 45 °C for 30 min may be used to investigate complaints about performance at low temperatures.

LEGAL REQUIREMENTS. “Standard” diesel fuel: CFPP at most 0 °C in the summer period (16.04–30.09), −10 °C in the transitional period (1.03–15.04 and 1.10–15.11) and −20 °C in the winter period (16.11–end of February); diesel fuel with improved low-temperature properties: at most −32 °C (Journal of Laws 2024, item 1018, Annex 3 item 19 and footnotes 3–5). Methyl ester used as a stand-alone fuel: 0, −10 and −20 °C in the same periods (Journal of Laws 2025, item 426, Annex 1 item 25).

WHAT WE DO NOT GIVE HERE. The publicly available text of the standard ends with the description of the pipette (6.5.1). We do not give the filter design, vacuum system, cooling baths and their temperatures, the course of the test (clauses 9–10), calibration (clause 11) or precision (clause 13).

Method principle

A test portion of the fuel is cooled under specified conditions and, at intervals of 1 °C, drawn into a pipette under a controlled vacuum of 2 kPa through a standardized wire mesh filter. When the separated wax crystals slow down the flow so that filling the pipette to the 20 ml mark takes longer than 60 s, or the fuel fails to return completely to the jar before cooling by a further 1 °C, the test ends; the temperature at which the last filtration was commenced is recorded as the CFPP (clause 4, 6.5.1).

Applications

Key parameters

ParameterValue
Definition of CFPPhighest temperature at which the fuel fails to pass through the filter in a specified time (3.1)
Temperature stepfiltration at every 1 °C (clause 4)
Vacuum2 kPa (clause 4)
Criterionfilling the 20 ml pipette takes longer than 60 s, or incomplete return of the fuel before cooling by a further 1 °C (clause 4, 6.5.1)
Test jarglass, outside diameter (34 ± 0.5) mm, height (120 ± 5) mm, 45 ml mark (6.1)
Equipment for referee purposesautomated only (clause 1)

Standard

Standard number
PN-EN 116:2015-09
Title (PL)
Oleje napędowe i oleje opałowe lekkie — Oznaczanie temperatury zablokowania zimnego filtru — Metoda stopniowego schładzania
Title (EN)
Diesel and domestic heating fuels — Determination of cold filter plugging point — Stepwise cooling bath method

Step-by-step procedure

  1. Sampling

    According to EN ISO 3170 or EN ISO 3171 (normative references).

  2. Filling the test jar

    The test jar is filled with sample to the 45 ml mark (6.1).

  3. Cooling and filtration at every 1 °C

    The fuel is cooled under specified conditions; at each further 1 °C it is drawn under a vacuum of 2 kPa through the filter into the pipette, and the time to fill it to the 20 ml mark is measured (clause 4, 6.5.1).

  4. End of the test

    The test ends when filling the pipette takes longer than 60 s or the fuel fails to return completely to the jar before it has cooled by a further 1 °C (clause 4).

  5. Result

    The indicated temperature at which the last filtration was commenced is recorded as the CFPP (clause 4). Preparation of the apparatus, the detailed procedure and the expression of results are in clauses 9, 10 and 12 of the standard, outside the publicly available text.

Required equipment and apparatus

EquipmentExampleIndicative price
Automated (or manual) apparatusarrangement as in Figure 1 of the standard; for referee purposes automated only; parts made of copper, zinc and brass can interact with FAME — parts of alternative materials are available (clauses 1, 6)—
Test jarcylindrical, clear glass, flat-bottomed, outside diameter (34 ± 0.5) mm, wall (1.25 ± 0.25) mm, height (120 ± 5) mm, permanent mark at 45 ml (6.1)—
Jacket and spacerwatertight cylindrical jacket (inside diameter (45 ± 0.25) mm, height (115 ± 3) mm) used as an air bath; spacer of polyoxymethylene copolymer with stainless steel rods (6.2–6.3)—
Stopperoil-resistant plastic, non-thermally-conductive material, with three holes — for the pipette, the thermometer and venting (6.4)—
Pipette with filter unitclear glass, mark (20 ± 0.2) ml at (149 ± 0.5) mm from the bottom, connected to the filter unit (6.5.1)—

Reagents, media and consumables

ReagentCASDetails
Hydrocarbon solvent—technical grade, e.g. heptane (5.1)
Light hydrocarbon solvent—technical grade, e.g. isopentane (5.2)
Lintless filter paper—with particle retention of (5 ± 1) µm (5.3)
Certified reference materials—e.g. from the European Commission’s Institute for Reference Materials and Measurements (IRMM) (5.4)

Health and safety (OHS)

Frequently asked questions

Which standard describes this test?

The test is performed according to PN-EN 116:2015-09 — “Diesel and domestic heating fuels — Determination of cold filter plugging point — Stepwise cooling bath method”.

How does this method work?

A test portion of the fuel is cooled under specified conditions and, at intervals of 1 °C, drawn into a pipette under a controlled vacuum of 2 kPa through a standardized wire mesh filter. When the separated wax crystals slow down the flow so that filling the pipette to the 20 ml mark takes longer than 60 s, or the fuel fails to return completely to the jar before cooling by a further 1 °C, the test ends; the temperature at which the last filtration was commenced is recorded as the CFPP (clause 4, 6.

What is the measuring range and accuracy?

Definition of CFPP: highest temperature at which the fuel fails to pass through the filter in a specified time (3.1); Temperature step: filtration at every 1 °C (clause 4); Vacuum: 2 kPa (clause 4); Criterion: filling the 20 ml pipette takes longer than 60 s, or incomplete return of the fuel before cooling by a further 1 °C (clause 4, 6.5.1).

How long does the test take?

The procedure comprises 5 steps. The standard does not give a duration for every stage — the laboratory's own procedure decides.

What equipment is required?

Automated (or manual) apparatus, Test jar, Jacket and spacer, Stopper, Pipette with filter unit.

Where is this test used?

Diesel fuel — CFPP at most 0 / −10 / −20 °C in the summer, transitional and winter periods; with improved low-temperature properties −32 °C (Journal of Laws 2024, item 1018); Methyl ester used as a stand-alone fuel — 0 / −10 / −20 °C (Journal of Laws 2025, item 426, Annex 1); Domestic heating fuels, distillate fuels, paraffinic diesel fuels, including those with FAME, flow improvers and other additives (clause 1); Investigating complaints about low-temperature performance — comparing the sample as received and after 30 min at 45 °C (clause 1).

What safety precautions apply?

The standard warns that its use can involve hazardous materials, operations and equipment, and that users ensure the safety and health of personnel before applying it (clause 1); Heptane and isopentane are flammable — according to their safety data sheets; Apparatus parts made of copper, zinc and brass can interact with FAME (clause 6).

Which laboratory can perform this test?

The test is performed by laboratories accredited to ISO/IEC 17025. On LabCoda you can find them by the standard number PN-EN 116.

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